This hypothesis is supported by the fact that use of carbon dioxide in the Parr bomb reduces the yield of N-ethylbenzylamine to negligible quantities. Of those tested, the two best methods of reduction, from. Synthesis Of Phenylacetone. The work of Jarowski and Hartung already has been mentioned 2. Preparation of 2-methylamino-1-phenyl-1-propanol Formaldehyde (0.3 mole of active material as 37 solution) was added, with cooling, to 2-amino-1-phenyl-1-propanol (45.3g, 0.3 mole) dissolved in.
The ethereal solution was dried over Drierite, and after removal of ether, distilled (bp 120-130C/2-4 mmHg) The usual conversion is 90-100g (50-55) and the yield, based on benzaldehyde which reacts, is nearly quantitative.
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